Spectroscopy in Catalysis. 3rd, Completely Revised and Enlarged Edition

  • ID: 2179724
  • Book
  • 344 Pages
  • John Wiley and Sons Ltd
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This third edition includes significant new developments and case studies,with all the chapters updated by way of recent examples and relevant new literature. For students and for everyone who wants a digestible introduction to catalyst characterization.

Superbly organized and of great pedagogic value, "Spectroscopy in Catalysis" describes the most important modern analytical techniques used to investigate catalytic surfaces. These include electron, ion, and vibrational spectroscopy, mass spectrometry, temperature–programmed techniques, diffraction, and microscopy. With the focus on practical use, rather than theory, each chapter presents current applications to illustrate the type of information that the technique provides and evaluates its possibilities and limitations, allowing selection of the best catalyst and the correct technique to solve a given problem.

From reviews of the previous editions:

This is a truly valuable book...very useful for industrial practitioners who need to be aware of the type of information that can be obtained from modern surface spectroscopies...The book has a superb pedagogic value..." (Journal of Catalysis)

"...this is an excellent text on spectroscopies in catalysis and I highly recommend it for...introductory courses on heterogeneous catalysis or as a general introductory monograph." (Journal of the American Chemical Society)

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INTRODUCTION

Heterogeneous Catalysis

The Aim of Catalyst Characterization

Spectroscopic Techniques

Research Strategies

TEMPERATURE–PROGRAMMED TECHNIQUES

Introduction

Temperature–Programmed Reduction

Temperature–Programmed Sulfidation

Temperature–Programmed Reaction Spectroscopy

Temperature–Programmed Desorption

Temperature–Programmed Reaction Spectroscopy in UHV

PHOTOEMISSION AND AUGER SPECTROSCOPY

Introduction

X–Ray Photoelectron Spectroscopy (XPS)

Ultraviolet Photoelectron Spectroscopy (UPS)

Auger Electron Spectroscopy

THE ION SPECTROSCOPIES

Introduction

Secondary Ion Mass Spectrometry (SIMS)

Secondary Neutral Mass Spectrometry (SNMS)

Ion Scattering: The Collision Process

Rutherford Backscattering Spectrometry (RBS)

Low–Energy Ion Scattering (LEIS)

MOESSBAUER SPECTROSCOPY

Introduction

The Moessbauer Effect

Moessbauer Spectroscopy

Moessbauer Spectroscopy in Catalyst Characterization

DIFFRACTION AND EXTENDED X–RAY ABSORPTION FINE STRUCTURE (EXAFS)

Introduction

X–Ray Diffraction

Low–Energy Electron Diffraction (LEED)

X–Ray Absorption Fine Structure (XAFS)

MICROSCOPY AND IMAGING

Introduction

Electron Microscopy

Field Emission Microscopy and Ion Microscopy

Scanning Probe Microscopy: AFM and STM

Other Imaging Techniques

VIBRATIONAL SPECTROSCOPY

Introduction

Theory of Molecular Vibrations

Infrared Spectroscopy

Sum–Frequency Generation

Raman Spectroscopy

Electron Energy Loss Spectroscopy (EELS)

CASE STUDIES IN CATALYST CHARACTERIZATION

Introduction

Supported Rhodium Catalysts

Alkali Promoters on Metal Surfaces

Cobalt–Molybdenum Sulfide Hydrodesulfurization Catalysts

Chromium Polymerization Catalysts

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J. W. Niemantsverdriet
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