ICP Emission Spectrometry

  • ID: 2183010
  • Book
  • 281 Pages
  • John Wiley and Sons Ltd
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All the fundamentals needed for successful ICP OES analyses.

Using a clear and comprehensive style, the author introduces practitioners to ICP emission spectrometry, covering the basics as well as information of device technology, instructions on how to develop methods and numerous concrete examples.

The layout is extremely reader–friendly and well structured, with the author highlighting typical questions and problems, while also providing checklists and detailed instructions for implementation.

Thus, this book is not intended merely for the readers′ own training and further education, but its sections on maintenance and troubleshooting also make it a reliable source for lab chemists.

Throughout, the author draws on his knowledge and experience gained over the last 20 years in developing devices for a leading manufacturer and in training and advising users as a freelance consultant. Knowledge now available to all users of ICP OES.

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OVERVIEW

Analytic features of the ICP OES

ICP OES – definitions

Distribution of the ICP emission spectrometers

Complimentary techniques for elemental analysis

Symbols, abbreviations and acronyms used

PLASMA

The analytically used plasma

Excitation to emit electromagnetic radiation

High–frequency generator

Sample introduction system

OPTICS AND DETECTOR OF THE SPECTROMETER

Principles of optics

Detector

Emission spectrometer mounts

METHOD DEVELOPMENT

Wavelength selection

Processing and correction techniques

Non–spectral interferences

Optimization

Validation

ROUTINE ANALYSIS

Preliminary steps

Calibration

Quality control

Software and data management

TROUBLE SHOOTING

APPLICATIONS

General Notes

Notes on specific elements

Selected applications

INSTRUMENT PURCHASING AND LABORATORY PREPARATION

Which technique in atomic spectrometry is preferred?

Which ICP emission spectrometer is best for the application?

Preparation of the laboratory

LITERATURE

INDEX

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Joachim Nölte
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