Practical Microwave Synthesis for Organic Chemists

  • ID: 2183197
  • Book
  • 310 Pages
  • John Wiley and Sons Ltd
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With the novice user in mind, this beginner`s guide explains the

basics behind microwave technology, evaluates available instruments

and reaction modes, and provides practical hints for every eventuality.

Includes 27 detailed protocols for often–used reactions.

From the contents:

1 Microwave Synthesis – An Introduction

2 Microwave Theory

3 Equipment Review

4 Microwave Processing Techniques

5 Starting With Microwave Chemistry

6 Experimental Protocols

6.1 General Small–Scale Sealed–Vessel Microwave Processing

6.2 Reaction Optimization

6.3 Library Generation

6.4 Reaction Scale–Up

6.5 Special Processing Techniques
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1 Microwave Synthesis –

An Introduction 1

2 Microwave Theory 11

3 Equipment Review 45

4 Microwave Processing Techniques 87

5 Starting With Microwave Chemistry 163

6 Experimental Protocols 205

6.1 General Small–Scale Sealed–Vessel Microwave Processing 207

6.2 Reaction Optimization 234

6.3 Library Generation 239

6.4 Reaction Scale–Up 251

6.5 Special Processing Techniques
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C. Oliver Kappe
Doris Dallinger
Shaun S. Murphree
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