Reactions and Syntheses. In the Organic Chemistry Laboratory. 2nd, Completely Revised and Updated Edition

  • ID: 2882912
  • Book
  • 668 Pages
  • John Wiley and Sons Ltd
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The second edition of this classic text book has been completely revised, updated, and extended to include chapters on biomimetic amination reactions, Wacker oxidation, and useful domino reactions.

The first–class author team with long–standing experience in practical courses on organic chemistry covers a multitude of preparative procedures of reaction types and compound classes indispensable in modern organic synthesis. Throughout, the experiments are accompanied by the theoretical and mechanistic fundamentals, while the clearly structured sub–chapters provide concise background information, retrosynthetic analysis, information on isolation and purification, analytical data as well as current literature citations. Finally, in each case the synthesis is labeled with one of three levels of dificulty.

An indispensable manual for students and lecturers in chemistry, organic chemists, as well as lab technicians and chemists in the pharmaceutical and agrochemical industries.
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C–C BOND FORMATION

Nucleophilic Addition to Aldehydes, Ketones, Carboxylic Acid Derivatives (Esters, Anhydrides) and alpha,beta–Unsaturated Carbonyl Compounds;

Carbonyl Olefination

Alkylation of Aldehydes/Ketones, Carboxylic Acids, and beta–Dicarbonyl Compounds

Reactions of the Aldol and Mannich Type

Electrophilic and Nucleophilic Acylation

Reactions of Alkenes via Carbenium Ions

Transition–Metal–Catalyzed Reactions

Pericyclic Reactions

Radical Reactions

OXIDATION AND REDUCTION

Epoxidation of C=C Bonds

Dihydroxylation of C=C Bonds

Oxidation of Alcohols to Carbonyl Compounds

Enantioselective Reduction of Ketones

Biomimetic Reductive Amination

Enantioselective Wacker

HETEROCYCLIC COMPOUNDS

Three– and Four–Membered Heterocycles

Five–Membered Heterocycles

Six–Membered Heterocycles

Condensed Heterocycles

Other Heterocyclic Systems;

Heterocyclic Dyes

SELECTED NATURAL PRODUCTS

Isoprenoids

Carbohydrates

Amino Acids and Peptides

Nucleotides and Oligonucleotides

DOMINO REACTIONS

Domino Reactions in Synthetic Methodology

Domino Reactions in The Synthesis of Alkaloids

Domino Reactions in The Synthesis of Isoprenoids

Domino Reactions for The Synthesis of Chromans And Dioxins

Domino Reactions in The Synthesis of Chiroptical Switches

INDEX OF REACTIONS

INDEX OF PRODUCTS

SUBJECT INDEX
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Lutz F. Tietze
Theophil Eicher
Ulf Diederichsen
Andreas Speicher
Nina Schützenmeister
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