A comprehensive guide on In situ Scanning transmission electron microscope with the basic principles and techniques and methodologies available (a) to carry out in situ/operando measurements of morphology, structure and chemical changes under different kinds of stimuli; (b) to measure electrical and mechanical properties at nanoscale; and (c) establish the relationship between morphology, structure, chemistry and property of nanomaterials. The book will show how existing methodologies function, how to modify them to suit a project, to design new experiments, limitations and future perspectives in the field. Each chapter will provide practical guidelines and hands on knowledge from experienced researchers through a textbook approach that will aid students and professionals to keep pace with the fast-developing field.
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Table of Contents
CHAPTER 1
INTRODUCTION
1.1 Scope of the Book
1.2 Review of the Chapters
CHAPTER 2
FUNDAMENTALS OF ELECTRON MICROSCOPY
2.1 Overview of Electron Optics
2.2 General functioning and applications of TEM/STEM
CHAPTER 3
IMPACT AND LIMITATIONS OF IN-SITU TECHNIQUES
3.1 Potential Benefits of Performing an In situ TEM experiment
3.2 Potential Limitations and Cautions of Performing an In situ TEM experiment
CHAPTER 4
GENERAL MICROSCOPE SELECTION AND STAGE DESIGN PHILOSOPHY
4.1 Microscope Selection
4.2 Stage Design Philosophy
4.3 Image Recording Techniques
CHAPTER 5
IN SITU DEFORMATION
5.1 Qualitative Loading
5.2 Quantitative Loading
CHAPTER 6
IN SITU HEATING
6.1 Classical Conductive Heating
6.2 MEMS Conductive Heating
6.3 Convective Heating
6.4 Radiative Heating
CHAPTER 7
IN SITU COOLING
7.1 Peltier Cooling
7.2 Cryogenic Cooling
CHAPTER 8
IN SITU CHARGED PARTICLE RADIATION
8.1 Electron Irradiation
8.2 Ion Irradiation
CHAPTER 9
IN-SITU GAS-SOLID REACTIONS
9.1 Environmental Stages
9.2 Environmental Microscopes
CHAPTER 10
IN SITU LIQUID-SOLID INTERACTIONS
10.1 Ionic Liquids and Closed Liquid Cell
10.2 Microfluidic Design
Chapter 11
IN SITU EM FIELD EFFECTS
11.1 Electrical Biasing
11.2 Dynamic Lorentz Imaging
Chapter 12
DYNAMIC AND ULTRA-FAST TEM
12.1 Dynamic TEM
12.2 Ultra-fast TEM
CHAPTER 13
COUPLING OF IN SITU TEM TECHNIQUES
13.1 Coupling within the listed approaches
13.2 Coupling to other Structure and Property
CHAPTER 14
DATA HANDLING AND PROCESSING
14.1 Data Collection
14.2 Data Processing
14.3 Data Storage
CHAPTER 15
FUTURE DIRECTION OF IN SITU TEM TECHNIQUES
15.1 Future direction in Hardware
15.2 Future Direction in Software
CHAPTER 16
Summary
Appendix A: Glossary
Appendix B: List of Suppliers
Acknowledgements
References
CHAPTER 1
INTRODUCTION
1.1 Scope of the Book
1.2 Review of the Chapters
CHAPTER 2
FUNDAMENTALS OF ELECTRON MICROSCOPY
2.1 Overview of Electron Optics
2.2 General functioning and applications of TEM/STEM
CHAPTER 3
IMPACT AND LIMITATIONS OF IN-SITU TECHNIQUES
3.1 Potential Benefits of Performing an In situ TEM experiment
3.2 Potential Limitations and Cautions of Performing an In situ TEM experiment
CHAPTER 4
GENERAL MICROSCOPE SELECTION AND STAGE DESIGN PHILOSOPHY
4.1 Microscope Selection
4.2 Stage Design Philosophy
4.3 Image Recording Techniques
CHAPTER 5
IN SITU DEFORMATION
5.1 Qualitative Loading
5.2 Quantitative Loading
CHAPTER 6
IN SITU HEATING
6.1 Classical Conductive Heating
6.2 MEMS Conductive Heating
6.3 Convective Heating
6.4 Radiative Heating
CHAPTER 7
IN SITU COOLING
7.1 Peltier Cooling
7.2 Cryogenic Cooling
CHAPTER 8
IN SITU CHARGED PARTICLE RADIATION
8.1 Electron Irradiation
8.2 Ion Irradiation
CHAPTER 9
IN-SITU GAS-SOLID REACTIONS
9.1 Environmental Stages
9.2 Environmental Microscopes
CHAPTER 10
IN SITU LIQUID-SOLID INTERACTIONS
10.1 Ionic Liquids and Closed Liquid Cell
10.2 Microfluidic Design
Chapter 11
IN SITU EM FIELD EFFECTS
11.1 Electrical Biasing
11.2 Dynamic Lorentz Imaging
Chapter 12
DYNAMIC AND ULTRA-FAST TEM
12.1 Dynamic TEM
12.2 Ultra-fast TEM
CHAPTER 13
COUPLING OF IN SITU TEM TECHNIQUES
13.1 Coupling within the listed approaches
13.2 Coupling to other Structure and Property
CHAPTER 14
DATA HANDLING AND PROCESSING
14.1 Data Collection
14.2 Data Processing
14.3 Data Storage
CHAPTER 15
FUTURE DIRECTION OF IN SITU TEM TECHNIQUES
15.1 Future direction in Hardware
15.2 Future Direction in Software
CHAPTER 16
Summary
Appendix A: Glossary
Appendix B: List of Suppliers
Acknowledgements
References
Note: Product cover images may vary from those shown
Khalid Hattar
Renu Sharma
Renu Sharma
Note: Product cover images may vary from those shown
